
Expedition Five flight engineer Peggy Whitson is shown installing the Solidification Using a Baffle in Sealed Ampoules (SUBSA) experiment in the Microgravity Science Glovebox (MSG) in the Destiny laboratory aboard the International Space Station (ISS). SUBSA examines the solidification of semiconductor crystals from a melted material. Semiconductor crystals are used for many products that touch our everyday lives. They are found in computer chips, integrated circuits, and a multitude of other electronic devices, such as sensors for medical imaging equipment and detectors of nuclear radiation. Materials scientists want to make better semiconductor crystals to be able to further reduce the size of high-tech devices. In the microgravity environment, convection and sedimentation are reduced, so fluids do not remove and deform. Thus, space laboratories provide an ideal environment of studying solidification from the melt. This investigation is expected to determine the mechanism causing fluid motion during production of semiconductors in space. It will provide insight into the role of the melt motion in production of semiconductor crystals, advancing our knowledge of the crystal growth process. This could lead to a reduction of defects in semiconductor crystals produced in space and on Earth.

Marshall graduate student researcher Juliana Neves, who is pursuing her doctorate in civil engineering at Pennsylvania State University, monitors cement paste samples returned from space as part of the Microgravity Investigation of Cement Solidification. Neves, investigators at Penn State and Marshall researchers led by NASA materials scientist Richard Grugel mirrored each sample experiment conducted on the International Space Station -- 120 tests on the ground, 120 in orbit -- and will continue to assess their findings in months to come.

The Advanced Automated Directional Solidification Furnace (AADSF) with the Experimental Apparatus Container (EAC) removed flew during the USMP-2 mission. During USMP-2, the AADSF was used to study the growth of mercury cadmium telluride crystals in microgravity by directional solidification, a process commonly used on earth to process metals and grow crystals. The furnace is tubular and has three independently controlled temperature zones . The sample travels from the hot zone of the furnace (1600 degrees F) where the material solidifies as it cools. The solidification region, known as the solid/liquid interface, moves from one end of the sample to the other at a controlled rate, thus the term directional solidification.

The Advanced Automated Directional Solidification Furnace (AADSF) flew during the USMP-2 mission. During USMP-2, the AADSF was used to study the growth of mercury cadmium telluride crystals in microgravity by directional solidification, a process commonly used on earth to process metals and grow crystals. The furnace is tubular and has three independently controlled temperature zones. The sample travels from the hot zone of the furnace (1600 degrees F) where the material solidifies as it cools. The solidification region, known as the solid/liquid interface, moves from one end of the sample to the other at a controlled rate, thus the term directional solidification.

iss038e045758 (2/12/2014) --- A view of Columnar-to-Equiaxed Transition in Solidification Processing-2 (CETSOL-2) test sample 7 which is to be installed into the Material Science Laboratory (MSL) Solidification and Quench Furnace (SQF). This investigation aims to deepen the understanding of the physical principles that govern solidification processes in metal alloys. The patterns of the crystals resulting from transitions of liquids to solids is important for processes used to produce materials such as solar cells, thermoelectrics, and metal alloys.

iss038e045760 92/12/2014) --- A view of Columnar-to-Equiaxed Transition in Solidification Processing-2 (CETSOL-2) test sample 7 which is to be installed into the Material Science Laboratory (MSL) Solidification and Quench Furnace (SQF). This investigation aims to deepen the understanding of the physical principles that govern solidification processes in metal alloys. The patterns of the crystals resulting from transitions of liquids to solids is important for processes used to produce materials such as solar cells, thermoelectrics, and metal alloys.

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). A technician is working on the Advanced Automated Directional Solidification Furnace (AADSF), which will be used by researchers to study the solidification of semiconductor materials in microgravity. Scientists will be able to better understand how microgravity influences the solidification process of these materials and develop better methods for controlling that process during future Space flights and Earth-based production. All STS-87 experiments are scheduled for launch on Nov. 19 from KSC

Technicians are monitoring experiments on the United States Microgravity Payload-4 (USMP-4) in preparation for its scheduled launch aboard STS-87 on Nov. 19 from Kennedy Space Center (KSC). USMP-4 experiments are prepared in the Space Station Processing Facility at KSC. The large white vertical cylinder in the center of the photo is the Advanced Automated Directional Solidification Furnace (AADSF), which is a sophisticated materials science facility used for studying a common method of processing semiconductor crystals called directional solidification. The white horizontal tube to the right is the Isothermal Dendritic Growth Experiment (IDGE), which will be used to study the dendritic solidification of molten materials in the microgravity environment

Test Engineer, Ron Cantrell loads the sample in the (AADSF) Advanced Automated Directional Solidification Furnace.

Peter Curerri with KC-135 experiment hardware, a prototype aircraft version of Advanced Automated Directional Solidification Furnace (AADSF).

Advanced Automated Directional Solidification Furnace (AADSF) G-Cel with Fred Flack and Wayne Gandy in the Microgravity Development Laboratory clean room.

Evolution of Furnaces for Crystal Growth. Left view: Crystal Growth Furnace (CGF) Right view: Advanced Automated Directional Solidification Furnace (AADSF)

iss057e106264 (Nov. 27, 2018) --- Flight Engineer Serena Auñón-Chancellor mixes samples for the Microgravity Investigation of Cement Solidification (MICS) experiment and installs them into the Multi-use Variable-g Platform. The research utilizes the microgravity environment aboard the International Space Station to investigate the complex process of cement solidification. Results may impact possible construction processes and designs for space habitats on the surface of the Moon and Mars.

The purpose of the experiments for the Advanced Automated Directional Solidification Furnace (AADSF) is to determine how gravity-driven convection affects the composition and properties of alloys (mixtures of two or more materials, usually metal). During the USMP-4 mission, the AADSF will solidify crystals of lead tin telluride and mercury cadmium telluride, alloys of compound semiconductor materials used to make infrared detectors and lasers, as experiment samples. Although these materials are used for the same type application their properties and compositional uniformity are affected differently during the solidification process.

iss057e106256 (Nov. 27, 2018) --- NASA astronaut Serena Auñón-Chancellor mixes samples for the Microgravity Investigation of Cement Solidification (MICS) experiment and installs them into the Multi-use Variable-g Platform. The research utilizes the microgravity environment aboard the International Space Station to investigate the complex process of cement solidification. Results may impact possible construction processes and designs for space habitats on the surface of the Moon and Mars.

The MEPHISTO experiment is a cooperative American and French investigation of the fundamentals of crystal growth. MEPHISTO is a French-designed and built materials processing furnace. MEPHISTO experiments study solidation (also called freezing) during the growth cycle of liquid materials used for semiconductor crystals. Solidification is the process where materials change from liquid (melt) to solid. An example of the solidification process is water changing into ice.

iss057e106244 (Nov. 27, 2018) --- NASA astronaut Serena Auñón-Chancellor mixes samples for the Microgravity Investigation of Cement Solidification (MICS) experiment and installs them into the Multi-use Variable-g Platform. The research utilizes the microgravity environment aboard the International Space Station to investigate the complex process of cement solidification. Results may impact possible construction processes and designs for space habitats on the surface of the Moon and Mars.

iss057e106250 (Nov. 27, 2018) --- NASA astronaut Serena Auñón-Chancellor mixes samples for the Microgravity Investigation of Cement Solidification (MICS) experiment and installs them into the Multi-use Variable-g Platform. The research utilizes the microgravity environment aboard the International Space Station to investigate the complex process of cement solidification. Results may impact possible construction processes and designs for space habitats on the surface of the Moon and Mars.

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). Seen in the foreground at left is the USMP-4 logo with the acronyms of its experiments. Above the American flag at left is the MEPHISTO experiment, a cooperative American and French investigation of the fundamentals of crystal growth. The large white vertical cylinder in the center of the photo is the Advanced Automated Directional Solidification Furnace (AADSF), which is a sophisticated materials science facility used for studying a common method of processing semiconductor crystals called directional solidification. The white horizontal tube to the right is the Isothermal Dendritic Growth Experiment (IDGE), which will be used to study the dendritic solidification of molten materials in the microgravity environment. All USMP-4 experiments are scheduled for launch aboard STS-87 on Nov. 19 from KSC

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). The vertical tube in the center of the photo is the Advanced Automated Directional Solidification Furnace (AADSF), which will be used by researchers to study the solidification of semiconductor materials in microgravity. Scientists will be able to better understand how microgravity influences the solidification process of these materials and develop better methods for controlling that process during future Space flights and Earth-based production. To its left is MEPHISTO, the French acronym for a cooperative American-French investigation of the fundamentals of crystal growth. All STS-87 experiments are scheduled for launch on Nov. 19 from KSC
Impact crater floors are commonly flat and relatively smooth, the result of the cooling and solidification of impact melt generated by the impact event itself. Often, the pool of impact melt cracks as it cools, a process well illustrated by the striking Abedin crater. Although not visible in the frame above, this crater also hosts cooling cracks on its floor. It also boasts numerous terraces along its inner wall, which likely formed after the impact melt solidified. Note how the fine-grained texture of the inner walls contrasts with the crater's floor. http://photojournal.jpl.nasa.gov/catalog/PIA19231

Jeri Briscoe of the video team inspects the optical system for proper alignment during a test run of the Equiaxed Dendritic Solidification Experiment (EDSE) located in the Microgravity Development Laboratory (MDL).

Typical metal sample that was processed by TEMPUS (Tiegelfreies Elektromagnetisches Prozessieren Unter Schwerelosigkeit), an electromagnetic levitation facility developed by German researchers and flown on the IML-2 and MSL-1 and 1R Spacelab missions. Electromagnetic levitation is used commonly in ground-based experiments to melt and then cool metallic melts below their freezing points without solidification occurring. Sample size is limited in ground-based experiments. Research with TEMPUS aboard Spacelab allowed scientists to study the viscosity, surface tension, and other properties of several metals and alloys while undercooled (i.e., cooled below their normal solidification points). The sample is about 1 cm (2/5 inch) in diameter.

Technicians are monitoring experiments on the United States Microgravity Payload-4 (USMP-4) in preparation for its scheduled launch aboard STS-87 on Nov. 19 from Kennedy Space Center (KSC). USMP-4 experiments are prepared in the Space Station Processing Facility at KSC. The large white vertical cylinder at the right of the photo is the Advanced Automated Directional Solidification Furnace (AADSF ), which is a sophisticated materials science facility used for studying a common method of processing semiconductor crystals called directional solidification. The technician in the middle of the photo is leaning over MEPHISTO, a cooperative American-French investigation of the fundamentals of crystal growth
Video images sent to the ground allow scientists to watch the behavior of the bubbles as they control the melting and freezing of the material during the Pore Formation and Mobility Investigation (PFMI) in the Microgravity Science Glovebox aboard the International Space Station. While the investigation studies the way that metals behave at the microscopic scale on Earth -- and how voids form -- the experiment uses a transparent material called succinonitrile that behaves like a metal to study this problem. The bubbles do not float to the top of the material in microgravity, so they can study their interactions.

iss057e092614 (11/14/2018) --- Photo documentation of the Kobairo Rack front, JPM1F3 in the Kibo Japanese Experiment Module (JEM) aboard the International Space Staion (ISS). The KOBAIRO Rack houses the Gradient Heating Furnace (GHF), an experiment facility for investigating crystal growth of semiconductors. This furnace has the capability of directional solidification of samples.

iss042e049014 (12/18/2014) --- A view of the interior of the Kobairo rack of the Japanese Experiment Module (JEM) aboard the International Space station (ISS).The KOBAIRO Rack houses the Gradient Heating Furnace (GHF), an experiment facility for investigating crystal growth of semiconductors. This furnace has the capability of directional solidification of samples.

ISS026-E-014925 (4 Jan. 2011) --- NASA astronaut Catherine (Cady) Coleman, Expedition 26 flight engineer, removes the Low Gradient Furnace (LGF) and installs the Solidification and Quench Furnace (SQF) in the Material Science Laboratory (MSL) in the Destiny laboratory of the International Space Station.

iss066e044525 (Nov. 4, 2021) --- NASA astronaut and Expedition 66 Flight Engineer Mark Vande Hei works inside the Microgravity Science Glovebox setting up hardware for a space physics study, known as Solidification Using a Baffle in Sealed Ampoules (SUBSA), seeking to improve the production of higher quality semiconductor crystals.

iss059e027344 (April 19, 2019) --- Astronaut David Saint-Jacques of the Canadian Space Agency studies how crystals melt and solidify using the Microgravity Science Glovebox inside the U.S. Destiny laboratory module. The Solidification Using a Baffle in Sealed Ampoules study explores how to produce high-quality semi-conductor crystals in microgravity.

iss065e020575 (May 6, 2021) --- NASA astronaut and Expedition 65 Flight Engineer Shane Kimbrough sets up the U.S. Destiny laboratory module's Microgravity Science Glovebox for a physics investigation. The study known as Solidification Using a Baffle in Sealed Ampoules, or SUBSA, explores improving technology used in producing semiconductor crystals.

iss070e001580 (10/2/2023) --- A aboard the International Space Station (ISS) of the Transparent Alloys hardware installed into the Microgravity Science Glovebox (MSG) with a sample cartridge. Transparent Alloys consists of numerous experiments to study various growth and solidification processes in alloys.

iss065e073965 (May 26, 2021) --- Expedition 65 Commander Akihiko Hoshide of the Japan Aerospace Exploration Agency checks out hardware for a physics experiment also known as SUBSA, or Solidification Using a Baffle in Sealed Ampoules. The space physics study is exploring ways to improve the production of semiconductor crystals.

ISS026-E-014915 (4 Jan. 2011) --- NASA astronaut Catherine (Cady) Coleman, Expedition 26 flight engineer, removes the Low Gradient Furnace (LGF) and installs the Solidification and Quench Furnace (SQF) in the Material Science Laboratory (MSL) in the Destiny laboratory of the International Space Station.

ISS026-E-014918 (4 Jan. 2011) --- NASA astronaut Catherine (Cady) Coleman, Expedition 26 flight engineer, removes the Low Gradient Furnace (LGF) and installs the Solidification and Quench Furnace (SQF) in the Material Science Laboratory (MSL) in the Destiny laboratory of the International Space Station.

iss065e021208 (May 6, 2021) --- Roscosmos cosmonaut and Expedition 65 Flight Engineer Oleg Novitskiy swaps hardware inside the U.S. Destiny laboratory module's Microgravity Science Glovebox for a physics investigation. The study known as Solidification Using a Baffle in Sealed Ampoules, or SUBSA, explores improving technology used in producing semiconductor crystals.

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). The large white vertical cylinder in the center of the photo is the Advanced Automated Directional Solidification Furnace (AADSF) and the horizontal tube to the left of it is MEPHISTO, a French acronym for a cooperative American-French investigation of the fundamentals of crystal growth. Seen at right behind the AADSF in the circular white cover is the Isothermal Dendritic Growth Experiment (IDGE), which will be used to study the dendritic solidification of molten materials in the microgravity environment. Under the multi-layer insulation with the American flag and mission logo is the Space Acceleration Measurement System, or SAMS, which measures the microgravity conditions in which the experiments are conducted. All of these experiments are scheduled for launch aboard STS-87 on Nov. 19 from KSC

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). The large white vertical cylinder in the middle of the photo is the Advanced Automated Directional Solidification Furnace (AADSF) and the horizontal tube to its left is MEPHISTO, the French acronym for a cooperative American-French investigation of the fundamentals of crystal growth. Seen to the right of the AADSF is the Isothermal Dendritic Growth Experiment (IDGE), which will be used to study the dendritic solidification of molten materials in the microgravity environment. Under the multi-layer insulation with the American flag and mission logo is the Space Acceleration Measurement System, or SAMS, which measures the microgravity conditions in which the experiments are conducted. All of these experiments are scheduled for launch aboard STS-87 on Nov. 19 from KSC

TEMPUS, an electromagnetic levitation facility that allows containerless processing of metallic samples in microgravity, first flew on the IML-2 Spacelab mission. The principle of electromagnetic levitation is used commonly in ground-based experiments to melt and then cool metallic melts below their freezing points without solidification occurring. The TEMPUS operation is controlled by its own microprocessor system; although commands may be sent remotely from the ground and real time adjustments may be made by the crew. Two video cameras, a two-color pyrometer for measuring sample temperatures, and a fast infrared detector for monitoring solidification spikes, will be mounted to the process chamber to facilitate observation and analysis. In addition, a dedicated high-resolution video camera can be attached to the TEMPUS to measure the sample volume precisely.

ISS034-E-040265 (5 Feb. 2013) --- Canadian Space Agency astronaut Chris Hadfield, Expedition 34 flight engineer, holds two Material Science Laboratory Solidification and Quench Furnace (MSL SQF) Sample Cartridge Mechanical Protection Containers (MPCs), during MSL Sample Cartridge Exchange, in the Destiny laboratory of the International Space Station.
jsc2021e029751 (7/15/2021) --- A diagram showing the the Process cycle of the Electromagnetic Levitator (EML) - Batch 3 of samples. EML is a multi-user facility that provides containerless melting and solidification of electrically conductive, spherical samples, under ultra-high vacuum and/or high gas-purity conditions. Heating and positioning of the sample is achieved by electromagnetic fields generated by a coil system. Batch 3 is a new Sample Chamber to be mounted to the EML process chamber, bringing 18 new samples

The Equiaxed Dendritic Solidification Experiment (EDSE) is a material sciences investigation under the Formation of Microstructures/pattern formation discipline. The objective is to study the microstructural evolution of and thermal interactions between several equiaxed crystals growing dendritically in a supercooled melt of a pure and transparent substance under diffusion controlled conditions. This image shows the overview for the EDSE in the Microgravity Development Lab (MDL).

iss005e06782 (7/5/2002) --- NASA astronaut Peggy Whitson installs a Solidification Using a Baffle in Sealed Ampoules (SUBSA) Process Control Module in the Microgravity Science Glovebox (MSG). The SUBSA objective is to advance our understanding of the processes involved in semiconductor crystal growth. It offers a gradient freeze furnace for materials science investigations that can reach 850°C. Samples are contained in transparent quartz or ceramic ampoules with high definition video imaging available in real-time along with remote commanding of thermal control parameters.

The Equiaxed Dendritic Solidification Experiment (EDSE) is a material sciences investigation under the Formation of Microstructures/pattern formation discipline. The objective is to study the microstructural evolution of and thermal interactions between several equiaxed crystals growing dendritically in a supercooled melt of a pure and transparent substance under diffusion controlled conditions. Video and power rack for the EDSE in the Microgravity Development Lab (MDL).

iss065e084906 (June 1, 2021) --- Expedition 65 Flight Engineer Thomas Pesquet of ESA (European Space Agency) swaps samples inside the Microgravity Sciences Glovebox for an experiment called Solidification Using a Baffle in Sealed Ampoules, or SUBSA. The physics investigation explores experimental methods of crystallizing melts in microgravity and is expected to result in reduced fluid motion in the melt, leading to better distribution of subcomponents and the potential for improved technology used in producing semiconductor crystals.

ISS005-E-06787 (5 July 2002) --- Astronaut Peggy A. Whitson, Expedition Five flight engineer, works near the Microgravity Science Glovebox (MSG) in the Destiny laboratory on the International Space Station (ISS). Whitson spent much of the morning installing the Solidification Using a Baffle in Sealed Ampoules (SUBSA) experiment in the MSG. The SUBSA installation will be completed once the MSG is activated.

iss058e028142 (3/7/2019) --- View of the Microgravity Sciences Glovebox (MSG) during configuration of the SUBSA (Solidification Using Baffles in Sealed Ampoules) hardware in the MSG Work Volume in the Destiny Laboratory aboard the International Space Staion(ISS). SUBSA is a high-temperature furnace that can be used to study how microgravity affects the synthesis of semiconductor and scintillator crystals.

The M512 Materials Processing Facility (MPF) with the M518 Multipurpose Electric Facility (MEF) tested and demonstrated a facility approach for materials process experimentation in space. It also provided a basic apparatus and a common interface for a group of metallic and nonmetallic materials experiments. The MPF consisted of a vacuum work chamber and associated mechanical and electrical controls. The M518 Multipurpose Electric Furnace (MEF) was an electric furnace system in which solidification, crystal growth, and other experiments involving phase changes were performed.

iss064e032426 (Feb. 12, 2021) --- NASA astronaut and Expedition 64 Flight Engineer Michael Hopkins swaps samples inside the Microgravity Science Glovebox for the SUBSA (Solidification Using Baffles in Sealed Ampoules) experiment. The SUBSA physics study explores experimental methods of crystallizing melts in microgravity that may contribute to the production of higher quality semiconductor crystals.

Test engineers, TK Pedergrass and Dave McIntosh, are growing multiple dendrites in an undercooled melt of ultra pure succinonitrile (SCN). Images and temperature measurements will give Dr. Christoph Beckerman, the EDSE Principal Investigator, information on the microstructural evolution of and thermal interactions between several equiaxed crystals growing dendritically. This benchmark data will be used to test and develop equiaxed dendritic solidification models. The monitors show both the 4 stinger and 2 stinger chambers that are placed in the isothermal bath for testing.

The Equiaxed Dendritic Solidification Experiment (EDSE) is a material sciences investigation under the Formation of Microstructures/pattern formation discipline. The objective is to study the microstructural evolution of and thermal interactions between several equiaxed crystals growing dendritically in a supercooled melt of a pure and transparent substance under diffusion controlled conditions. EDSE/TDSE project engineer, Zena Hester, monitors a test run of the EDSE located in the Microgravity Development Laboratory (MDL).

STS078-368-022 (20 June - 7 July 1996) --- Astronauts Susan J. Helms, payload commander, and Terence T. (Tom) Henricks, mission commander, prepare a sample cartridge containing semiconductor crystals for Spacelab research. The crystals were later placed in the Advanced Gradient Heating Furnace (AGHF) in the Life and Microgravity Spacelab (LMS-1) Science Module. The AGHF is designed for directional solidification of the crystals in the sample cartridges. The microgravity of space allows the crystals to grow in a perfect state that can not be accomplished in Earth's gravity.

iss066e078285 (Nov. 17, 2021) --- International Space Station Commander Anton Shkaplerov of Roscosmos (from left) and NASA astronaut and Expedition 66 Flight Engineer Thomas Marshburn work on the SUBSA-BRAINS (BRazing of Aluminum alloys IN Space) space physics experiment taking place inside the Microgravity Science Glovebox. The study examines differences in capillary flow, interface reactions, and bubble formation during solidification of brazing alloys in microgravity.

iss065e061407 (May 24, 2021) --- NASA astronaut and Expedition 65 Flight Engineer Megan McArthur works in the Microgravity Science Glovebox swapping samples for an experiment called Solidification Using a Baffle in Sealed Ampoules, or SUBSA. The physics investigation explores experimental methods of crystallizing melts in microgravity and is expected to result in reduced fluid motion in the melt, leading to better distribution of subcomponents and the potential for improved technology used in producing semiconductor crystals.

The Equiaxed Dendritic Solidification Experiment (EDSE) is a material sciences investigation under the Formation of Microstructures/pattern formation discipline. The objective is to study the microstructural evolution of and thermal interactions between several quiaxed crystals growing dendritically in a supercooled melt of a pure and transparent substance under diffusion controlled conditions. George Myers, controls engineer, monitors the thermal environment of a ground test for the EDSE located in the Microgravity Development Laboratory (MDL).

iss056e073250 (July 2, 2018) --- Astronaut Alexander Gerst of ESA (European Space Agency) works on the Microgravity Investigation of Cement Solidification (MICS) 2 experiment aboard the International Space Station. MICS 2 is researching how cement reacts in space during the hardening process and may help engineers better understand its microstructure and material properties. Observations could improve cement processing techniques on Earth and lead to the design of safer, lightweight space habitats.

iss066e078283 (Nov. 17, 2021) --- International Space Station Commander Anton Shkaplerov of Roscosmos works on the SUBSA-BRAINS (BRazing of Aluminum alloys IN Space) space physics experiment taking place inside the Microgravity Science Glovebox. The study examines differences in capillary flow, interface reactions, and bubble formation during solidification of brazing alloys in microgravity.

The Equiaxed Dendritic Solidification Experiment (EDSE) is a material sciences investigation under the Formation of Microstructures/pattern formation discipline. The objective is to study the microstructural evolution of and thermal interactions between several equiaxed crystals growing dendritically in a supercooled melt of a pure and transparent substance under diffusion controlled conditions. Dendrites growing at .4 supercooling from a 2 stinger growth chamber for the EDSE in the Microgravity Development Lab (MDL).

The Equiaxed Dendritic Solidification Experiment (EDSE) is a material sciences investigation under the Formation of Microstructures/pattern formation discipline. The objective is to study the microstructural evolution of and thermal interactions between several equiaxed crystals growing dendritically in a supercooled melt of a pure and transparent substance under diffusion controlled conditions. This image shows the isothermal bath and video system for the EDSE in the Microgravity Development Lab (MDL).

iss065e050120 (May 21, 2021) --- NASA astronaut and Expedition 65 Flight Engineer Shane Kimbrough swaps samples inside the Microgravity Science Glovebox for an experiment called Solidification Using a Baffle in Sealed Ampoules, or SUBSA. The physics investigation explores experimental methods of crystallizing melts in microgravity and is expected to result in reduced fluid motion in the melt, leading to better distribution of subcomponents and the potential for improved technology used in producing semiconductor crystals.

iss064e016385 (Dec. 29, 2020) --- NASA astronaut and Expedition 64 Flight Engineer Shannon Walker sets up hardware inside the Microgravity Science Glovebox for the Solidification Using a Baffle in Sealed Ampoules (SUBSA) experiment. SUBSA crystallizes melts in microgravity to learn more about the process of semiconductor crystal growth to benefit Earth and space industries. Results may lead to reduced fluid motion in the melt, leading to better distribution of subcomponents and the potential for improved technology used in producing semiconductor crystals.

iss065e020580 (May 5, 2021) --- NASA astronaut and Expedition 65 Flight Engineer Shane Kimbrough is pictured in front of the Microgravity Science Glovebox setting up hardware for a physics investigation. The experiment known as Solidification Using a Baffle in Sealed Ampoules, or SUBSA, explores experimental methods of crystallizing melts in microgravity and is expected to result in reduced fluid motion in the melt, leading to better distribution of subcomponents and the potential for improved technology used in producing semiconductor crystals.

iss066e078282 (November 17, 2021) --- NASA astronaut Tom Marshburn works on the SUBSA-BRAINS space physics experiment, which examines differences in capillary flow, interface reactions, and bubble formation during solidification of brazing alloys in microgravity. Brazing technology bonds similar materials (such as an aluminum alloy to aluminum) or dissimilar ones (such as aluminum alloy to ceramics) at temperatures above 450°C. It is a potential tool for construction of human space habitats and manufactured systems as well as to repair damage from micrometeoroids or space debris.

iss056e037491 (June 26, 2018) --- Astronaut Serena Auñón-Chancellor from NASA works on the Microgravity Investigation of Cement Solidification (MICS) 2 experiment aboard the International Space Station. MICS 2 is researching how cement reacts in space during the hardening process and may help engineers better understand its microstructure and material properties. Observations could improve cement processing techniques on Earth and lead to the design of safer, lightweight space habitats.

The Equiaxed Dendritic Solidification Experiment (EDSE) is a material sciences investigation under the Formation of Microstructures/pattern formation discipline. The objective is to study the microstructural evolution of and thermal interactions between several equiaxed crystals growing dendritically in a supercooled melt of a pure and transparent substance under diffusion controlled conditions. Dendrite irritator control for the EDSE in the Microgravity Development Lab (MDL).

iss056e073247 (July 2, 2018) --- Astronaut Alexander Gerst of ESA (European Space Agency) works on the Microgravity Investigation of Cement Solidification (MICS) 2 experiment aboard the International Space Station. MICS 2 is researching how cement reacts in space during the hardening process and may help engineers better understand its microstructure and material properties. Observations could improve cement processing techniques on Earth and lead to the design of safer, lightweight space habitats.

jsc2020e030481 (7/8/2020) --- This preflight image of the Dendrite Fragmentation and Morphology during Melting and Solidification (DFM) (SUBSA-DFM) investigation of shows a small portion of an experimentally determined dendrite. The image on the right shows the same portion with the formation of a fragment and other morphological changes after a simulated temperature change. Colors show the mean curvature of the dendrite interfaces (red corresponds to high positive curvature, blue to high negative curvature, and green to zero curvature). (Image Courtesy Techshot, Inc.)

iss073e0002997 (4/28/2025) --- A view of the Colloidal Solids investigation inside the Microgravity Sciences Glovebox (MSG). Colloidal Solids (COLIS) provides researchers with a better understanding of the origin, formation, and dynamics of protein crystals and colloidal glasses and gels. COLIS is a state-of-the-art multi-line light scattering apparatus that enables the research team to monitor the dynamics of physical processes, during and after solidification, of soft matter solids on the International Space Station (ISS) to assess the role played by gravity on the properties of growing structures.

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). Seen in the foreground at right is the Isothermal Dendritic Growth Experiment (IDGE), which will be used to study the dendritic solidification of molten materials in the microgravity environment. The metallic breadbox-like structure behind the IDGE is the Confined Helium Experiment (CHeX) that will study one of the basic influences on the behavior and properties of materials by using liquid helium confined between solid surfaces and microgravity. The large white vertical cylinder at left is the Advanced Automated Directional Solidification Furnace (AADSF) and the horizontal tube behind it is MEPHISTO, the French acronym for a cooperative American-French investigation of the fundamentals of crystal growth. Just below the left end of MEPHISTO is the Space Acceleration Measurement System, or SAMS, which measures the microgravity conditions in which the experiments are conducted. All of these experiments are scheduled for launch aboard STS-87 on Nov. 19 from KSC

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). Seen at right in the circular white cover is the Isothermal Dendritic Growth Experiment (IDGE), which will be used to study the dendritic solidification of molten materials in the microgravity environment. The large white vertical cylinder in the center of the photo is the Advanced Automated Directional Solidification Furnace (AADSF) and the horizontal tube to the left of it is MEPHISTO, a French acronym for a cooperative American-French investigation of the fundamentals of crystal growth. Just below MEPHISTO is the Space Acceleration Measurement System, or SAMS, which measures the microgravity conditions in which the experiments are conducted. The The metallic breadbox-like structure behind the AADSF is the Confined Helium Experiment (CHeX) that will study one of the basic influences on the behavior and properties of materials by using liquid helium confined between solid surfaces and microgravity. All of these experiments are scheduled for launch aboard STS-87 on Nov. 19 from KSC

While the microgravity environment of orbit eliminates a number of effects that impede the formation of materials on Earth, the change can also cause new, unwanted effects. A mysterious phenomenon, known as detached solidification, apparently stems from a small hydrostatic force that turns out to be pervasive. The contact of the solid with the ampoule transfers stress to the growing crystal and causing unwanted dislocations and twins. William Wilcox and Liya Regel of Clarkson University theorize that the melt is in contact with the ampoule wall, while the solid is not, and the melt and solid are cornected by a meniscus. Their work is sponsored by NASA's Office of Biological and Physical Researcxh, and builds on earlier work by Dr. David Larson of the State University of New York at Stony Brook.

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). This horizontal tube is known as MEPHISTO, the French acronym for a cooperative American-French investigation of the fundamentals of crystal growth. This experiment, designed for the study of solidification (or freezing) during the growth cycle of liquid materials used for semiconductor crystals, aims to aid in the development of techniques for growing higher quality crystals on Earth. All STS-87 experiments are scheduled for launch on Nov. 19 from KSC

iss055e005543 (March 26, 2018) --- Expedition 55 Flight Engineer and astronaut Scott Tingle is pictured conducting the Transparent Alloys experiment inside the Destiny lab module's Microgravity Science Glovebox. The Transparent Alloys study is a set of five experiments that seeks to improve the understanding of melting-solidification processes in plastics without the interference of Earth's gravity environment. Results may impact the development of new light-weight, high-performance structural materials for space applications. Observations may also impact fuel efficiency, consumption and recycling of materials on Earth potentially reducing costs and increasing industrial competitiveness.

As a liquefied metal solidifies, particles dispersed in the liquid are either pushed ahead of or engulfed by the moving solidification front. Similar effects can be seen when the ground freezes and pushes large particles out of the soil. The Particle Engulfment and Pushing (PEP) experiment, conducted aboard the fourth U.S. Microgravity Payload (USMP-4) mission in 1997, used a glass and plastic beads suspended in a transparent liquid. The liquid was then frozen, trapping or pushing the particles as the solidifying front moved. This simulated the formation of advanced alloys and composite materials. Such studies help scientists to understand how to improve the processes for making advanced materials on Earth. The principal investigator is Dr. Doru Stefanescu of the University of Alabama. This image is from a video downlink.

STS026-06-018 (29 Sept. - 3 Oct. 1988) --- Astronaut John M. Lounge, STS-26 mission specialist (MS), using a beverage container, experiments with microgravity as Commander Frederick H. Hauck (left) and MS David C. Hilmers (right) look on. Lounge freefloats as he closes in on a sphere of the red liquid drifting in front of his mouth. Hauck holds a spoon while sipping from a beverage container as he balances a meal tray assembly on his thighs. Hilmers, partially blocked by the open airlock hatch and holding a spoon and a can of food, pauses to watch the experiment. Automated Directional Solidification Furnace (ADSF) and forward middeck lockers appear on Lounge's right.

iss056e131400 (7/31/2018) --- NASA astronaut Serena Auñón-Chancellor conducts research operations for the AngieX Cancer Therapy study inside the Microgravity Science Glovebox. The new cancer research seeks to test a safer, more effective treatment that targets tumor cells and blood vessels. In the background, NASA astronaut Drew Feustel can be seen working on the Microgravity Investigation of Cement Solidification (MICS) 2 experiment aboard the International Space Station. MICS 2 is researching how cement reacts in space during the hardening process and may help engineers better understand its microstructure and material properties.

Angie Jackman, a NASA project manager in microgravity research, demonstrates the enhanced resilience of undercooled metal alloys as compared to conventional alloys. Experiments aboard the Space Shuttle helped scientists refine their understanding of the physical properties of certain metal alloys when undercooled (i.e., kept liquid below their normal solidification temperature). This new knowledge then allowed scientists to modify a terrestrial production method so they can now make limited quantities marketed under the Liquid Metal trademark. The exhibit was a part of the NASA outreach activity at AirVenture 2000 sponsored by the Experimental Aircraft Association in Oshkosh, WI.

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). Seen in the foreground at right is the Isothermal Dendritic Growth Experiment (IDGE), which will be used to study the dendritic solidification of molten materials in the microgravity environment. The metallic breadbox-like structure behind the IDGE is the Confined Helium Experiment (CHeX) that will study one of the basic influences on the behavior and properties of materials by using liquid helium confined between solid surface, and microgravity. These experiments are scheduled for launch aboard STS-87 on Nov. 19 from KSC

ss038e008298 (11/26/2013) --- A view of NASA astronaut Rick Mastracchio, during the Material Science Laboratory (MSL) Solidification and Quench Furnace (SQF) Sample Cartridge Exchange aboard the International Space Station (ISS). The Materials Science Laboratory (MSL) is used for basic materials research in the microgravity environment of the ISS. The MSL can accommodate and support diverse Experiment Modules. In this way many material types, such as metals, alloys, polymers, semiconductors, ceramics, crystals, and glasses, can be studied to discover new applications for existing materials and new or improved materials.

iss056e131403 (7/31/2018) --- NASA astronaut Serena Auñón-Chancellor conducts research operations for the AngieX Cancer Therapy study inside the Microgravity Science Glovebox. The new cancer research seeks to test a safer, more effective treatment that targets tumor cells and blood vessels. In the background, NASA astronaut Drew Feustel can be seen working on the Microgravity Investigation of Cement Solidification (MICS) 2 experiment aboard the International Space Station. MICS 2 is researching how cement reacts in space during the hardening process and may help engineers better understand its microstructure and material properties.

ISS036-E-034881 (20 Aug. 2013) --- European Space Agency astronaut Luca Parmitano, Expedition 36 flight engineer, works with Microgravity Science Laboratory (MSL) hardware in the Destiny laboratory of the International Space Station.

This computer-generated image depicts the Materials Science Research Rack-1 (MSRR-1) being developed by NASA's Marshall Space Flight Center and the European Space Agency (ESA) for placement in the Destiny laboratory module aboard the International Space Station. The rack is part of the plarned Materials Science Research Facility (MSRF) and is expected to include two furnace module inserts, a Quench Module Insert (being developed by NASA's Marshall Space Flight Center) to study directional solidification in rapidly cooled alloys and a Diffusion Module Insert (being developed by the European Space Agency) to study crystal growth, and a transparent furnace (being developed by NASA's Space Product Development program). Multi-user equipment in the rack is being developed under the auspices of NASA's Office of Biological and Physical Research (OBPR) and ESA. Key elements are labeled in other images (0101754, 0101829, 0101830).

Composite of Marshall Space Flight Center's Low-Gravity Free Fall Facilities.These facilities include a 100-meter drop tower and a 100-meter drop tube. The drop tower simulates in-flight microgravity conditions for up to 4.2 seconds for containerless processing experiments, immiscible fluids and materials research, pre-flight hardware design test and flight experiment simulation. The drop tube simulates in-flight microgravity conditions for up to 4.6 seconds and is used extensively for ground-based microgravity convection research in which extremely small samples are studied. The facility can provide deep undercooling for containerless processing experiments that require materials to remain in a liquid phase when cooled below the normal solidification temperature.

Representatives of NASA materials science experiments supported the NASA exhibit at the Rernselaer Polytechnic Institute's Space Week activities, April 5 through 11, 1999. From left to right are: Angie Jackman, project manager at NASA's Marshall Space Flight Center for dendritic growth experiments; Dr. Martin Glicksman of Rennselaer Polytechnic Instutute, Troy, NY, principal investigator on the Isothermal Dendritic Growth Experiment (IDGE) that flew three times on the Space Shuttle; and Dr. Matthew Koss of College of the Holy Cross in Worcester, MA, a co-investigator on the IDGE and now principal investigator on the Transient Dendritic Solidification Experiment being developed for the International Space Station (ISS). The image at far left is a dendrite grown in Glicksman's IDGE tests aboard the Shuttle. Glicksman is also principal investigator for the Evolution of Local Microstructures: Spatial Instabilities of Coarsening Clusters.

This scale model depicts the Materials Science Research Rack-1 (MSRR-1) being developed by NASA's Marshall Space Flight Center and the European Space Agency (ESA) for placement in the Destiny laboratory module aboard the International Space Station. The rack is part of the plarned Materials Science Research Facility (MSRF) and is expected to include two furnace module inserts, a Quench Module Insert (being developed by NASA's Marshall Space Flight Center) to study directional solidification in rapidly cooled alloys and a Diffusion Module Insert (being developed by the European Space Agency) to study crystal growth, and a transparent furnace (being developed by NASA's Space Product Development program). Multi-user equipment in the rack is being developed under the auspices of NASA's Office of Biological and Physical Research (OBPR) and ESA. Key elements are labeled in other images (0101754, 0101829, 0101830, and TBD). This image is from a digital still camera; higher resolution is not available.

This scale model depicts the Materials Science Research Rack-1 (MSRR-1) being developed by NASA's Marshall Space Flight Center and the European Space Agency (ESA) for placement in the Destiny laboratory module aboard the International Space Station. The rack is part of the plarned Materials Science Research Facility (MSRF) and is expected to include two furnace module inserts, a Quench Module Insert (being developed by NASA's Marshall Space Flight Center) to study directional solidification in rapidly cooled alloys and a Diffusion Module Insert (being developed by the European Space Agency) to study crystal growth, and a transparent furnace (being developed by NASA's Space Product Development program). Multi-user equipment in the rack is being developed under the auspices of NASA's Office of Biological and Physical Research (OBPR) and ESA. Key elements are labeled in other images (0101754, 0101829, 0101830, and TBD).

This scale model depicts the Materials Science Research Rack-1 (MSRR-1) being developed by NASA's Marshall Space Flight Center and the European Space Agency (ESA) for placement in the Destiny laboratory module aboard the International Space Station. The rack is part of the plarned Materials Science Research Facility (MSRF) and is expected to include two furnace module inserts, a Quench Module Insert (being developed by NASA's Marshall Space Flight Center) to study directional solidification in rapidly cooled alloys and a Diffusion Module Insert (being developed by the European Space Agency) to study crystal growth, and a transparent furnace (being developed by NASA's Space Product Development program). Multi-user equipment in the rack is being developed under the auspices of NASA's Office of Biological and Physical Research (OBPR) and ESA. Key elements are labeled in other images (0101754, 0101829, and TBD). This composite is from a digital still camera; higher resolution is not available.

One of the first materials science experiments on the International Space Station -- the Solidification Using a Baffle in Sealed Ampoules (SUBSA) -- will be conducted during Expedition Five inside the Microgravity Science Glovebox. The glovebox is the first dedicated facility delivered to the Station for microgravity physical science research, and this experiment will be the first one operated inside the glovebox. The glovebox's sealed work environment makes it an ideal place for the furnace that will be used to melt semiconductor crystals. Astronauts can change out samples and manipulate the experiment by inserting their hands into a pair of gloves that reach inside the sealed box. Dr. Aleksandar Ostrogorsky, a materials scientist from the Rensselaer Polytechnic Institute, Troy, N.Y., and the principal investigator for the SUBSA experiment, uses the gloves to examine an ampoule like the ones used for his experiment inside the glovebox's work area. The Microgravity Science Glovebox and the SUBSA experiment are managed by NASA's Marshall Space Flight Center in Huntsville, Ala.

The Transient Dendritic Solidification Experiment (TDSE) is being developed as a candidate for flight aboard the International Space Station. TDSE will study the growth of dendrites (treelike crystalline structures) in a transparent material (succinonitrile or SCN) that mimics the behavior or widely used iron-based metals. Basic work by three Space Shuttle missions of the Isothermal Dendritic Growth Experiment (IDGE) is yielding new insights into virtually all industrially relevant metal and alloy forming operations. The TDSE is similar to IDGE, but will maintain a constant temperature while varying pressure on the dendrites. Shown here is an exploded view of major elements of the TDSE. A similar view is availble without labels. The principal investigator is Matthew Koss of College of the Holy Cross in Worcester, MA. Photo credit: NASA/Marshall Space Flight Center (MSFC)

This scale model depicts the Materials Science Research Rack-1 (MSRR-1) being developed by NASA's Marshall Space Flight Center and the European Space Agency (ESA) for placement in the Destiny laboratory module aboard the International Space Station. The rack is part of the plarned Materials Science Research Facility (MSRF) and is expected to include two furnace module inserts, a Quench Module Insert (being developed by NASA's Marshall Space Flight Center) to study directional solidification in rapidly cooled alloys and a Diffusion Module Insert (being developed by the European Space Agency) to study crystal growth, and a transparent furnace (being developed by NASA's Space Product Development program). Multi-user equipment in the rack is being developed under the auspices of NASA's Office of Biological and Physical Research (OBPR) and ESA. Here the transparent furnace is extracted for servicing. Key elements are labeled in other images (0101754, 0101829, 0101830, and TBD).

The Transient Dendritic Solidification Expepriment (TDSE) is being developed as a candidate for flight aboard the International Space Station. TDSE will study the growth of dendrites (treelike crystalline structures) in a transparent material (succinonitrile or SCN) that mimics the behavior of widely used iron-based metals. Basic work by three Space Shuttle missions of the Isothermal Dendritic Growth Expepriment (IDGE) is yielding new insights into virtually all industrially relevant metal and alloy forming operations. The TDSE is similar to IDGE, but will maintain a constant temperature while varying pressure on the dendrites. Shown here is an exploded view of major elements of TDSE. A similar view is available with labels. The principal investigator is Matthew Koss of College of the Holy Cross in Worcester, MA. Photo credit: NASA/Marshall Space Flight Center (MSFC)

The Transient Dentritic Solidification Experiment (TDSE) is being developed as a candidate for flight aboard the International Space Station. TDSE will study the growth of dentrites (treelike crystalline structures) in a transparent material (succinonitrile or SCN) that mimics the behavior of widely used iron-based metals. Basic work by three Space Shuttle flights (STS-62, STS-75, and STS-87) of the Isothermal Dendritic Growth Experiment (IDGE) is yielding new insights into virtually all industrially relevant metal and alloy forming operations. The TDSE is similar to IDGE, but will maintain a constant temperature while varying pressure on the dentrites. Shown here is a cutaway of the isothermal bath containing its growth cell at the heart of the TDSE. The principal investigator is Matthew Koss of College of the Holy Cross in Worcester, MA. Note: an Acrobat PDF version is available from http://microgravity.nasa.gov/gallery

This metal sample, which is approximately 1 cm in diameter, is typical of the metals that were studied using the German designed electromagnetic containerless processing facility. The series of experiments that use this device is known as TEMPUS which is the acronym that stands for the German Tiegelfreies Elektromanetisches Prozessieren Unter Schwerelosigkeit. Most of the TEMPUS experiments focused on various aspects of undercooling liquid metal and alloys. Undercooling is the process of melting a material and then cooling it to a temperature that is below its normal freezing or solidification point. The TEMPUS experiments that used the metal cages as shown in the photograph, often studied bulk metallic glass, a solid material with no crystalline structures. We study metals and alloys not only to build things in space, but to improve things that are made on Earth. Metals and alloys are everywhere around us; in our automobiles, in the engines of aircraft, in our power-plants, and elsewhere. Despite their presence in everyday life, there are many scientific aspects of metals that we do not understand.

An entranced youngster watches a demonstration of the enhanced resilience of undercooled metal alloys as compared to conventional alloys. Steel bearings are dropped onto plates made of steel, titanium alloy, and zirconium liquid metal alloy, so-called because its molecular structure is amorphous and not crystalline. The bearing on the liquid metal plate bounces for a minute or more longer than on the other plates. Experiments aboard the Space Shuttle helped scientists refine their understanding of the physical properties of certain metal alloys when undercooled (i.e., kept liquid below their normal solidification temperature). This new knowledge then allowed scientists to modify a terrestrial production method so they can now make limited quantities marketed under the Liquid Metal trademark. The exhibit was a part of the NASA outreach activity at AirVenture 2000 sponsored by the Experimental Aircraft Association in Oshkosh, WI.

This computer-generated image depicts the Materials Science Research Rack-1 (MSRR-1) being developed by NASA's Marshall Space Flight Center and the European Space Agency (ESA) for placement in the Destiny laboratory module aboard the International Space Station. The rack is part of the plarned Materials Science Research Facility (MSRF) and is expected to include two furnace module inserts, a Quench Module Insert (being developed by NASA's Marshall Space Flight Center) to study directional solidification in rapidly cooled alloys and a Diffusion Module Insert (being developed by the European Space Agency) to study crystal growth, and a transparent furnace (being developed by NASA's Space Product Development program). Multi-user equipment in the rack is being developed under the auspices of NASA's Office of Biological and Physical Research (OBPR) and ESA. Key elements are labeled in other images (0101754, 0101830, and TBD).

United States Microgravity Payload-4 (USMP-4) experiments are prepared to be flown on Space Shuttle mission STS-87 in the Space Station Processing Facility at Kennedy Space Center (KSC). Seen in the foreground at right is the USMP-4 logo with the acronyms of its experiments. Above the American flag at left is the MEPHISTO experiment, a cooperative American and French investigation of the fundamentals of crystal growth. Scientists will study changes in solidification rates, temperature, and interface shape of an alloy to understand how these changes affect composition and properties of the metal produced. Under the multi-layer insulation with the American flag and mission logo is the Space Acceleration Measurement System, or SAMS, which measures the microgravity conditions in which the experiments are conducted. All USMP-4 experiments are scheduled for launch aboard STS-87 on Nov. 19 from KSC
This computer-generated image depicts the Materials Science Research Rack-1 (MSRR-1) being developed by NASA's Marshall Space Flight Center and the European Space Agency (ESA) for placement in the Destiny laboratory module aboard the International Space Station. The rack is part of the plarned Materials Science Research Facility (MSRF) and is expected to include two furnace module inserts, a Quench Module Insert (being developed by NASA's Marshall Space Flight Center) to study directional solidification in rapidly cooled alloys and a Diffusion Module Insert (being developed by the European Space Agency) to study crystal growth, and a transparent furnace (being developed by NASA's Space Product Development program). Multi-user equipment in the rack is being developed under the auspices of NASA's Office of Biological and Physical Research (OBPR) and ESA. A larger image is available without labels (No. 0101755).

This scale model depicts the Materials Science Research Rack-1 (MSRR-1) being developed by NASA's Marshall Space Flight Center and the European Space Agency (ESA) for placement in the Destiny laboratory module aboard the International Space Station. The rack is part of the plarned Materials Science Research Facility (MSRF) and is expected to include two furnace module inserts, a Quench Module Insert (being developed by NASA's Marshall Space Flight Center) to study directional solidification in rapidly cooled alloys and a Diffusion Module Insert (being developed by the European Space Agency) to study crystal growth, and a transparent furnace (being developed by NASA's Space Product Development program). Multi-user equipment in the rack is being developed under the auspices of NASA's Office of Biological and Physical Research (OBPR) and ESA. Key elements are labeled in other images (0101754, 0101829, 0101830, and TBD). This image is from a digital still camera; higher resolution is not available.

This is a Space Shuttle Columbia (STS-52) onboard photograph of the United States Microgravity Payload-1 (USMP-1) in the cargo bay. The USMP program is a series of missions developed by NASA to provide scientists with the opportunity to conduct research in the unique microgravity environment of the Space Shuttle's payload bay. The USMP-1 mission was designed for microgravity experiments that do not require the hands-on environment of the Spacelab. Science teams on the ground would remotely command and monitor instruments and analyze data from work stations at NASA's Spacelab Mission Operation Control facility at the Marshall Space Flight Center (MSFC). The USMP-1 payload carried three investigations: two studied basic fluid and metallurgical processes in microgravity, and the third would characterize the microgravity environment onboard the Space Shuttle. The three experiments that made up USMP-1 were the Lambda Point Experiment, the Space Acceleration Measurement System, and the Materials for the Study of Interesting Phenomena of Solidification Earth and in Orbit (MEPHISTO). The three experiments were mounted on two cornected Mission Peculiar Equipment Support Structures (MPESS) mounted in the orbiter's cargo bay. The USMP program was managed by the MSFC and the MPESS was developed by the MSFC.

This is a computer generated model of a ground based casting. The objective of the therophysical properties program is to measure thermal physical properties of commercial casting alloys for use in computer programs that predict soldification behavior. This could reduce trial and error in casting design and promote less scrap, sounder castings, and less weight. In order for the computer models to reliably simulate the details of industrial alloy solidification, the input thermophysical property data must be absolutely reliable. Recently Auburn University and TPRL Inc. formed a teaming relationship to establish reliable measurement techniques for the most critical properties of commercially important alloys: transformation temperatures, thermal conductivity, electrical conductivity, specific heat, latent heat, density, solid fraction evolution, surface tension, and viscosity. A new initiative with the American Foundrymens Society has been started to measure the thermophysical properties of commercial ferrous and non-ferrous casting alloys and make the thermophysical property data widely available. Development of casting processes for the new gamma titanium aluminide alloys as well as existing titanium alloys will remain a trial-and-error procedure until accurate thermophysical properties can be obtained. These molten alloys react with their containers on earth and change their composition - invalidating the measurements even while the data are being acquired in terrestrial laboratories. However, measurements on the molten alloys can be accomplished in space using freely floating droplets which are completely untouched by any container. These data are expected to be exceptionally precise because of the absence of impurity contamination and buoyancy convection effects. Although long duration orbital experiments will be required for the large scale industrial alloy measurement program that results from this research, short duration experiments on NASA's KC-135 low-g aircraft are already providing preliminary data and experience.